2,4,6-Trichloroiodobenzene

Izabela Kania-Korwel, Larry W. Robertson, Hans Joachim Lehmler, Scan Parkin

Research output: Contribution to journalArticlepeer-review

1 Scopus citations

Abstract

The crystal structure of 2,4,6-trichloroiodobenzene, C6H 2Cl3I, a precursor of polychlorinated biphenyls (PCB), was investigated. The 2,4,6-trichloroiodobenzene crystals were obtained while attempting to synthesize 2,2′,4,4′,6,6′-hexachlorobiphenyl using a Suzuki coupling reaction. While the 2,4,5-trichloroiodobenzene isomer was extensively disordered in the crystalline state, the title compound was well ordered. White needles were found to form upon recrystallization from methanol.

Original languageEnglish
Pages (from-to)o1770-o1771
JournalActa Crystallographica Section E: Structure Reports Online
Volume59
Issue number11
DOIs
StatePublished - Nov 2003

ASJC Scopus subject areas

  • Chemistry (all)
  • Materials Science (all)
  • Condensed Matter Physics

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