TY - JOUR
T1 - 3,4′,5-Trichlorobiphenyl-4-yl 2,2,2-trichloroethyl sulfate
AU - Lehmler, Hans Joachim
AU - He, Xianran
AU - Duffel, Michael W.
AU - Parkin, Sean
PY - 2013/4
Y1 - 2013/4
N2 - Crystals of the title compound, C14H8Cl6O 4S, are twinned by inversion, with unequal components [0.85 (3):0.15 (3)]. The asymmetric unit contains two independent molecules that are related by a pseudo-inversion center. The Car-O [1.393 (9) and 1.397 (9) Å] and ester S-O bond lengths [1.600 (5) and 1.590 (5) Å] of both molecules are comparable to the structurally related 2,3,5,5-trichlorobiphenyl- 4-yl 2,2,2-trichloroethyl sulfate. The dihedral angles between the benzene rings in the two molecules are 37.8 (2) and 35.0 (2)°.
AB - Crystals of the title compound, C14H8Cl6O 4S, are twinned by inversion, with unequal components [0.85 (3):0.15 (3)]. The asymmetric unit contains two independent molecules that are related by a pseudo-inversion center. The Car-O [1.393 (9) and 1.397 (9) Å] and ester S-O bond lengths [1.600 (5) and 1.590 (5) Å] of both molecules are comparable to the structurally related 2,3,5,5-trichlorobiphenyl- 4-yl 2,2,2-trichloroethyl sulfate. The dihedral angles between the benzene rings in the two molecules are 37.8 (2) and 35.0 (2)°.
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U2 - 10.1107/S1600536813007976
DO - 10.1107/S1600536813007976
M3 - Article
C2 - 23634142
AN - SCOPUS:84875994575
SN - 1600-5368
VL - 69
SP - o620
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 4
ER -