Crystal structure of 4,5-bis(3,4,5-trimethoxyphenyl)-2H-1,2,3-triazole methanol monosolvate

Nikhil Reddy Madadi, Narsimha Reddy Penthala, Shobanbabu Bommagani, Sean Parkin, Peter A. Crooks

Research output: Contribution to journalArticlepeer-review

4 Scopus citations


The title compound, C20H23N3O6 CH3OH, was synthesized by [3 + 2] cycloaddition of (Z)-2,3-bis(3,4,5-trimethoxyphenyl)acrylonitrile with sodium azide and ammonium chloride in DMF/water. The central nitrogen of the triazole ring is protonated. The dihedral angles between the triazole ring and the 3,4,5-trimethoxyphenyl ring planes are 34.31(4) and 45.03(5)°, while that between the 3,4,5-trimethoxyphenyl rings is 51.87(5)°. In the crystal, the molecules, along with two methanol solvent molecules are linked into an R4 4(10) centrosymmetric dimer by N-H⋯O and O-H⋯N hydrogen bonds.

Original languageEnglish
Pages (from-to)o1128-o1129
JournalActa Crystallographica Section E: Structure Reports Online
Issue number10
StatePublished - Oct 1 2014


  • 1,2,3-triazole
  • crystal structure
  • hydrogen bonds

ASJC Scopus subject areas

  • Chemistry (all)
  • Materials Science (all)
  • Condensed Matter Physics


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