Abstract
The paper reports the effect of starting powder size and sintering temperature on the grain refining in spark plasma sintering Al2O3. It was found that the grain refining effect only occurred for the starting particles larger than a certain size. The grain size increased with increasing sintering temperature. The grain refining is likely caused by the rearrangement of dislocations through a thermo-mechanical fatigue process. It suggested that nanostructured alumina ceramics could be synthesized from micro-sized powders by optimizing the particle size and sintering temperature.
Original language | English |
---|---|
Pages (from-to) | 596-600 |
Number of pages | 5 |
Journal | Journal of Alloys and Compounds |
Volume | 622 |
DOIs | |
State | Published - Feb 15 2015 |
Bibliographical note
Funding Information:This work was financially supported by the National Scientific Foundation of US (CMMI 0800086 & 0800018), Chinese Nature Science Foundation (Grant No. 51402237 ), China Scholarship Council (Grant No. 2008629106 ), State Key Laboratory of Solidification Processing (Grant No. 82-TZ-2013 ) and the “111” Project (B08040).
Publisher Copyright:
© 2014 Published by Elsevier B.V.
Keywords
- AlO
- Microstructure refining
- Nanostructure
- Spark plasma sintering
ASJC Scopus subject areas
- Mechanics of Materials
- Mechanical Engineering
- Metals and Alloys
- Materials Chemistry