Involvement of Histidine and Tryptophan Residues of Glutamine Binding Protein in the Interaction with Membrane-Bound Components of the Glutamine Transport System of Escherichia coli

Arthur G. Hunt, Jen shiang Hong

Research output: Contribution to journalArticlepeer-review

13 Scopus citations

Abstract

We treated the glutamine binding protein with diethyl pyrocarbonate (DEPC) and N-bromosuccinimide (NBS) to modify respectively the sole histidine and tryptophan residues and examined the effect of these modifications on the ability of the binding protein to bind glutamine as well as the ability to restore glutamine transport in membrane vesicles of Escherichia coli. Under the conditions used, both DEPC and NBS markedly inhibited the ability to restore glutamine transport in vesicles without any significant effect on glutamine binding. Moreover, saturating quantities of glutamine had no protective effect on the inactivation of the binding protein by DEPC or NBS. Fluorometric measurement and amino acid analysis indicate that the inactivation of the binding protein in restoring vesicle transport by NBS can be attributed to the oxidation of a single tryptophan residue. Similar analysis and the inability of hydroxylamine to reverse the effect of DEPC indicate that the effects of DEPC can probably be attributed to alterations of the sole histidine and/or one or more lysine residues of the binding protein. We conclude that the glutamine binding protein possesses at least two largely nono-verlapping functional domains, one responsible for glutamine binding and the other for the interaction with the other components of the glutamine transport system.

Original languageEnglish
Pages (from-to)851-854
Number of pages4
JournalBiochemistry
Volume22
Issue number4
DOIs
StatePublished - 1983

Funding

FundersFunder number
National Institute of General Medical SciencesP01GM029853

    ASJC Scopus subject areas

    • Biochemistry

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