Microtomographic Analysis of Resin Composite Core Material Porosity

Howard Roberts, Rodrigo Fuentealba, John Brewster

Research output: Contribution to journalArticlepeer-review

Abstract

Purpose: To nondestructively evaluate the porosity of ten contemporary resin composite core materials using microtomographic (microCT) analysis. Material and methods: Resin composite core material samples (n = 12) including dual-cure, visible light cure only, and a self-cure material were fabricated using a standardized mold following manufacturer's recommendations. After storage in phosphate buffered saline for one week, specimens were analyzed using a microCT unit at 5.3-µm resolution over a rotational range of 360°. Image 3D recombination and analysis was accomplished using microCT software. Evaluated parameters included material volume investigated, closed pore number and volume, as well as closed pore percentage. Parameter mean values were evaluated with Kruskal-Wallis/Dunn at a 95% confidence level (α = 0.05). Results: Mean percent total porosity with standard deviation identified significant differences in decreasing order as Ti-Core: 2.2 (0.4) > Ti-Core Auto E: 1.3 (0.3) = Ti-Core Flow Plus: 1.1 (0.02) > Clearfil Photo Core: 0.94 (0.5) = Clearfil DC Core Plus: 0.6 (0.18) = MultiCore Flow: 0.58 (0.1) > Fluorocore 2+: 0.14 (0.2) = Build-It FR: 0.068 (0.02) = Gradia Core: 0.03 (0.02) = Rebilda DC: 0.02 (0.01). A pilot microCT evaluation evaluating a mixing tip revealed incomplete mixture between the two resins with porosity introduced from turbulence as the materials are forced through the tip during preparation. Conclusions: A wide range of porosity was identified between the ten materials evaluated. These preliminary results warrant more investigation evaluating additional resin composite core materials, the preparation capabilities of automix tips, and porosity presence in the unmixed materials.

Original languageEnglish
Pages (from-to)623-630
Number of pages8
JournalJournal of Prosthodontics
Volume29
Issue number7
DOIs
StatePublished - Aug 1 2020

Bibliographical note

Publisher Copyright:
© 2020 by the American College of Prosthodontists

Funding

None of the authors declare any commercial interest or conflicts of interest in any of the products or techniques used in this study. Any opinions stated in this study are of the authors only and do not represent the official opinion of the United States Air Force, the Department of Defense, the Uniformed Services University of the Health Sciences, or the United States Government.

FundersFunder number
U.S. Department of Defense
U.S. Air Force
Uniformed Services University of the Health Sciences

    Keywords

    • Core material
    • MicroCT
    • Porosity
    • Resin composite

    ASJC Scopus subject areas

    • General Dentistry

    Fingerprint

    Dive into the research topics of 'Microtomographic Analysis of Resin Composite Core Material Porosity'. Together they form a unique fingerprint.

    Cite this