TY - JOUR
T1 - 3′,4′-Dichloro-biphenyl-4-yl 2,2,2-trichloroethyl sulfate
AU - Li, Xueshu
AU - Parkin, Sean
AU - Duffel, Michael W.
AU - Robertson, Larry W.
AU - Lehmler, Hans Joachim
PY - 2010
Y1 - 2010
N2 - The four independent molecules in the asymmetric unit of the title compound, C14H9Cl5O4S, are related by pseudo-inversion centres. The molecules have Caromatic-O bond lengths ranging from 1.426 (10) to 1.449 (9) Å and biphenyl-4-yl sulfate ester bond lengths ranging from 1.563 (6) to 1.586 (6) Å, which is comparable to structurally related sulfuric acid diesters. The dihedral angles between the benzene rings range from 22.5 (4) to 29.1 (4)° and are significantly smaller than the calculated dihedral angle of 41.2°.
AB - The four independent molecules in the asymmetric unit of the title compound, C14H9Cl5O4S, are related by pseudo-inversion centres. The molecules have Caromatic-O bond lengths ranging from 1.426 (10) to 1.449 (9) Å and biphenyl-4-yl sulfate ester bond lengths ranging from 1.563 (6) to 1.586 (6) Å, which is comparable to structurally related sulfuric acid diesters. The dihedral angles between the benzene rings range from 22.5 (4) to 29.1 (4)° and are significantly smaller than the calculated dihedral angle of 41.2°.
UR - https://www.scopus.com/pages/publications/77954420896
UR - https://www.scopus.com/inward/citedby.url?scp=77954420896&partnerID=8YFLogxK
U2 - 10.1107/S1600536810020362
DO - 10.1107/S1600536810020362
M3 - Article
C2 - 21587847
AN - SCOPUS:77954420896
SN - 1600-5368
VL - 66
SP - o1615-o1616
JO - Acta Crystallographica Section E: Structure Reports Online
JF - Acta Crystallographica Section E: Structure Reports Online
IS - 7
ER -